X-ray diffraction and diffusion (DRX)

Services and expertise

  • Diffraction intensities measurements on single crystals of small organic molecules and macromolecules (proteins, nucleic acids, complexes, supramolecular assemblies) : structure solution.
  • wide angle X-ray scattering (WAXS) experiments : powder and fiber diffraction

  • Single crystal studies can be achieve under cryo conditions (temperature range 100-400K).

  • Crystallization

Instruments

  • Microfocus rotating Cu anode Rigaku FRX 3kW (hybrid pixel detector Dectris Pilatus 200K).

  • Oxford Cryosystem 700 series.

  • SPTLabtech Mosquito (crystallization robot)

Access

For any analytical experiment with assistance, or for a R&D project, please ask the facility engineers for a detailed quotation.

Technical managers

Brice Kauffmann b.kauffmann@iecb.u-bordeaux.fr

Stéphane Massip   s.massip@iecb.u-bordeaux.fr

Scientific expertise

Gilles Guichard g.guichard@iecb.u-bordeaux.fr

Brice Kauffmann b.kauffmann@iecb.u-bordeaux.fr

 

Equipments

Rigaku FRX rotating anode

X-ray rotating anode Power : 3kW Osmic Varimax HF mirrors Partial Chi AFC10 goniometer

X-ray Diffraction and Diffusion

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Mosquito3 Crystallization robot

highly accurate and precise multi-channel pipetting from 500 nL to 5 µL Vapour diffusion in 96 well plates

Screening of crystallization conditions

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People

MASSIP Stéphane

UB engineer

KAUFFMANN Brice

CNRS research engineer

Latest publications

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